Sodium Hydroxide → Beta-D-Glucose 6-phosphate

HRID 256704

Reaktionsgleichung

Reaktionsgleichung von HRID 256704
[P:1]([O:5][CH2:6][C@@H:7]([OH:16])[C@@H:8]([OH:15])[C@H:9]([OH:14])[C@@H:10]([OH:13])[CH:11]=[O:12])([O-:4])([O-:3])=[O:2].[Ba+2].[OH-].[Na+].[BH4-].[Na+]>O>[CH2:6]([O:5][P:1]([OH:3])([OH:4])=[O:2])[C@H:7]1[O:16][C@@H:11]([OH:12])[C@H:10]([OH:13])[C@@H:9]([OH:14])[C@@H:8]1[OH:15]

Komponenten

5

Edukt 3

HCID 14798Sodium HydroxideHCID 111125Barium glucose 6-phosphateHCID 4311764Sodium borohydride

Produkt 1

HCID 439427Beta-D-Glucose 6-phosphate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Reaktionsbedingungen

Temperatur
45 °C

Versuchsvorschrift

To 10 ml of the aminated gel obtained in Preparation Example 2 were added, first 10 ml of water, next 1 g of barium glucose-6-phosphate, to which 0.5 ml of 2M NaOH was further added and the mixture was maintained at 45° C. for 1 hour. After 0.1 g of NaBH4 was added thereto, the mixture was allowed to stand at room temperature for 24 hours. After the reaction was completed, the gel was filtered off from the reaction mixture and washed with water to give a cellulose gel with immobilized glucose-6-phosphate. The amount of the introduced anionic functional group derived from the immobilized glucose-6-phosphate was 10 μmol to 1 ml of the adsorbent.

Aufarbeitung

  1. additionwere added
  2. filtrationthe gel was filtered off from the reaction mixture
  3. washwashed with water

Quellen und Nachweise

ORD-Eintrag
ord-bed67b7f3eff4616bf94a00e5dfb7fe8
Quelldatensatz
uspto-grants-1993_11
Patentnummer
US05258503

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