Ammonium Hydroxide → alpha-Amino-9H-xanthene-9-acetic acid

HRID 258190Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 258190
Cl.[NH2:2][CH:3]([CH:7]1[C:20]2[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=2[O:14][C:13]2[C:8]1=[CH:9][CH:10]=[CH:11][CH:12]=2)[C:4]([OH:6])=[O:5].[OH-].[NH4+]>O>[NH2:2][CH:3]([CH:7]1[C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][C:13]=2[O:14][C:15]2[C:20]1=[CH:19][CH:18]=[CH:17][CH:16]=2)[C:4]([OH:6])=[O:5]

Komponenten

4

Edukt 2

HCID 14923Ammonium HydroxideHCID 67805111alpha-Amino-9H-xanthene-9-acetic acid hydrochloride

Produkt 1

HCID 9816503alpha-Amino-9H-xanthene-9-acetic acid

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

α-Amino-9H-xanthene-9-acetic acid hydrochloride is dissolved in water and the pH of the solution is adjusted with dilute ammonium hydroxide solution to pH 7. The precipitate is collected by filtration, washed with water, boiled with water for a short time, cooled to room temperature, and collected to afford the title compound.

Aufarbeitung

  1. filtrationThe precipitate is collected by filtration
  2. washwashed with water
  3. customcollected

Quellen und Nachweise

ORD-Eintrag
ord-554525d0fffa4cb78e494cfa3229e3a3
Quelldatensatz
uspto-grants-1993_11
Patentnummer
US05264577

Notizen zur Reaktion

Wird geladen…