Hexafluoropropylene oxide → Perfluoro-2-methyl-3-oxaoctanedioyl fluoride

HRID 26670

Reaktionsgleichung

Reaktionsgleichung von HRID 26670
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Komponenten

5

Edukt 3

HCID 9883Hexafluoropropylene oxideHCID 25953Cesium fluorideHCID 21322078HCID 21322078, Verbindung

Produkt 1

HCID 13750853Perfluoro-2-methyl-3-oxaoctanedioyl fluoride

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 80711,2-DimethoxyethaneLösungsmittel

Versuchsvorschrift

In a 200 cc autoclave equipped with a mechanical stirrer, 5 g of cesium fluoride powder, 20 cc of ethyleneglycol dimethyl ether and 50 g of perfluoro-δ-valerolactone was charged. Thirty seven grams of hexafluoropropylene oxide was introduced intermittently into the reactor for about 2 hours with vigorously stirring at the temperature of 0° to 5° C. under a pressure of lower than 1.0 kg/cm2G.

Aufarbeitung

  1. customIn a 200 cc autoclave equipped with a mechanical stirrer

Quellen und Nachweise

ORD-Eintrag
ord-57aa123eba954a8f816580b55fae8e3e
Quelldatensatz
uspto-grants-1979_04
Patentnummer
US04151200

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