Anisole → N-(4-formyl-3-hydroxyphenyl)acetamide
Reaktionsgleichung
[C:1]1([O:7]C)C=CC=CC=1.[C:9]([NH:12][C:13]1[CH:14]=[C:15]([OH:19])[CH:16]=[CH:17][CH:18]=1)(=[O:11])[CH3:10]>>[OH:19][C:15]1[CH:14]=[C:13]([NH:12][C:9](=[O:11])[CH3:10])[CH:18]=[CH:17][C:16]=1[CH:1]=[O:7]Komponenten
3
Versuchsvorschrift
By operating according to Example 13, but using anisole as the solvent and a temperature of 100° C., and starting from 15.1 g of 3-acetylaminophenol, 9.0 g of a product (yield on the theoretical value=50%) having a melting point at 185°-186° C. were obtained.
Aufarbeitung
- customa temperature of 100° C.
- customyield on the theoretical value=50%)
- customat 185°-186° C.
- customwere obtained
Quellen und Nachweise
- ORD-Eintrag
- ord-21f595ce2255497e8b72055a7472fa8b
- Quelldatensatz
- uspto-grants-1979_04
- Patentnummer
- US04151201
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