Methacrylic Acid → Ethyl Methacrylate n-Butyl Methacrylate Ethylene Glycol Dimethacrylate Methacrylic Acid

HRID 323849

Reaktionsgleichung

Reaktionsgleichung von HRID 323849
CCCCCCCCCCCCOS([O-])(=O)=O.[Na+].S(OOS([O-])(=O)=O)([O-])(=O)=O.[Na+].[Na+].[C:31]([O:36][CH2:37][CH3:38])(=[O:35])[C:32]([CH3:34])=[CH2:33].[C:39]([O:44][CH2:45][CH2:46][CH2:47][CH3:48])(=[O:43])[C:40]([CH3:42])=[CH2:41].[C:49]([OH:54])(=[O:53])[C:50]([CH3:52])=[CH2:51].[C:55]([O:60][CH2:61][CH2:62][O:63][C:64](=[O:68])[C:65]([CH3:67])=[CH2:66])(=[O:59])[C:56]([CH3:58])=[CH2:57]>>[C:31]([O:36][CH2:37][CH3:38])(=[O:35])[C:32]([CH3:34])=[CH2:33].[C:39]([O:44][CH2:45][CH2:46][CH2:47][CH3:48])(=[O:43])[C:40]([CH3:42])=[CH2:41].[C:55]([O:60][CH2:61][CH2:62][O:63][C:64](=[O:68])[C:65]([CH3:67])=[CH2:66])(=[O:59])[C:56]([CH3:58])=[CH2:57].[C:49]([OH:54])(=[O:53])[C:50]([CH3:52])=[CH2:51]

Komponenten

7

Edukt 6

HCID 4093Methacrylic AcidHCID 7343Ethyl MethacrylateHCID 7354Butyl MethacrylateHCID 7355Ethylene glycol dimethacrylateHCID 62655Sodium PersulfateHCID 3423265Sodium Lauryl Sulfate

Produkt 1

HCID 131722115Ethyl Methacrylate n-Butyl Methacrylate Ethylene Glycol Dimethacrylate Methacrylic Acid

Versuchsvorschrift

Same as C5 except that the monomer emulsion was composed of 5 g of SDS, 1 g of sodium persulfate, 80 g of ethyl methacrylate, 100 g of n-butyl methacrylate, 10 g of methacrylic acid, and 10 g of ethylene glycol dimethacrylate. Glass transition temperature was 69° C., average final particle size was 39 nm and % solid was 20.9%.

Quellen und Nachweise

ORD-Eintrag
ord-4e9e712ef7cc464b8286e5878c77feae
Quelldatensatz
uspto-grants-2001_04
Patentnummer
US06214938B1

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