Hydrochloric Acid → 2-Acetylthio-3-methylbenzoic acid
Reaktionsgleichung
[SH:1][C:2]1[C:10]([CH3:11])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=[O:5].[C:12](OC(=O)C)(=[O:14])[CH3:13].Cl>C(O)(=O)C>[C:12]([S:1][C:2]1[C:10]([CH3:11])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=[O:5])(=[O:14])[CH3:13]Komponenten
5
Edukt 3
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
2-Mercapto-3-methylbenzoic acid (9.0 g, 54 mmol), acetic anhydride (6.5 g, 63 mmol) and glacial acetic acid (25 ml) were refluxed 1 hour, then poured into dilute hydrochloric acid. The product was filtered and recrystallized from toluene.
Aufarbeitung
- filtrationThe product was filtered
- customrecrystallized from toluene
Quellen und Nachweise
- ORD-Eintrag
- ord-6715ab2fd23843db950559761faa08af
- Quelldatensatz
- uspto-grants-1984_04
- Patentnummer
- US04440941
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