Formic Acid → HCID 178420610, Verbindung

HRID 33818

Reaktionsgleichung

Reaktionsgleichung von HRID 33818
[N:1]1[C:6](C=O)=[CH:5][CH:4]=[CH:3][C:2]=1C=O.[NH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.C(O)=O>C(O)C>[C:12]1([N:11]=[C:6]2[CH2:5][CH:4]=[CH:3][C:2](=[N:11][C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)[NH:1]2)[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Komponenten

5

Edukt 3

HCID 284Formic AcidHCID 6115AnilineHCID 794852,6-Diformylpyridine

Produkt 1

HCID 178420610HCID 178420610, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

2,6-pyridine dicarboxaldehyde (0.3071 g, 2.3 mmol) was added to a solution of aniline (0.5292 g, 5.7 mmol) in absolute ethanol (20 mL) at room temperature. 0.5 mL of formic acid was then added to the above solution. The mixture was stirred at room temperature for 65 hours. The product was filtered, washed with cold ethanol and dried in a vacuum oven (50° C.) overnight. Yield 0.2245 g (34.2%).

Aufarbeitung

  1. filtrationThe product was filtered
  2. washwashed with cold ethanol
  3. customdried in a vacuum oven (50° C.) overnight

Quellen und Nachweise

ORD-Eintrag
ord-21efaacccac443d7a83aa3e70255ab54
Quelldatensatz
uspto-grants-2008_09
Patentnummer
US07429684B2

Verknüpfte Notizen

Wird geladen…