Hydroxylamine → Benzohydroxamic acid

HRID 369479

Reaktionsgleichung

Reaktionsgleichung von HRID 369479
[NH2:1][OH:2].C(=O)([O-])O.[Na+].[C:8](Cl)(=[O:15])[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1>C(OCC)(=O)C>[C:8]([NH:1][OH:2])(=[O:15])[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1

Komponenten

5

Edukt 3

HCID 787HydroxylamineHCID 7412Benzoyl chlorideHCID 516892Sodium Bicarbonate

Produkt 1

HCID 10313Benzohydroxamic acid

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 8857Ethyl AcetateLösungsmittel

Versuchsvorschrift

To 156 mg of said compound (26) were added 3 ml of ethyl acetate, 3 ml of aqueous saturated sodium hydrogencarbonate, and 0.035 ml of benzoyl chloride and the mixture was reacted at room temperature for 3 hours to obtain a benzoylamino-alcohol compound (compound (27), C52H65NO14Si, molecular weight of 956.17).

Aufarbeitung

  1. customthe mixture was reacted at room temperature for 3 hours

Quellen und Nachweise

ORD-Eintrag
ord-6ec7d3c042fb4c9bb5df324eb6456e78
Quelldatensatz
uspto-grants-2000_10
Patentnummer
US06136990

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