Water → HCID 178419936, Verbindung

HRID 37455

Reaktionsgleichung

Reaktionsgleichung von HRID 37455
[C:1]([C:3]1[CH:12]=[CH:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=1)#[N:2].[N-:13]=[N+:14]=[N-:15].[Na+].[Cl-].[Li+].O>COCCO>[CH:4]1[C:5]2[C:10](=[CH:9][CH:8]=[CH:7][CH:6]=2)[CH:11]=[CH:12][C:3]=1[C:1]1[NH:15][N:14]=[N:13][N:2]=1

Komponenten

6

Edukt 4

HCID 962WaterHCID 119442-NaphthalenecarbonitrileHCID 33557Sodium AzideHCID 433294Lithium Chloride

Produkt 1

HCID 178419936HCID 178419936, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 80192-MethoxyethanolLösungsmittel

Versuchsvorschrift

A mixture of 10 g of 2-cyanonaphthalene, 10.61 g of sodium azide, and 7.67 g of lithium chloride was placed in a reaction vessel, and 240 ml of 2-methoxyethanol serving as a solvent was added thereto. The above mixture was refluxed with stirring for 80 hours. The mixture was cooled to room temperature, and 500 ml of water was added to the mixture.

Aufarbeitung

  1. customwas placed in a reaction vessel
  2. temperatureThe above mixture was refluxed

Quellen und Nachweise

ORD-Eintrag
ord-28f1ea35b4c54d3e98646f4aae82b802
Quelldatensatz
uspto-grants-1995_05
Patentnummer
US05420288

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