Sodium Iodide → HCID 66732740, Verbindung

HRID 389002

Reaktionsgleichung

Reaktionsgleichung von HRID 389002
[OH:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1.[I-].[Na+].[OH-].[Na+].Cl[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][OH:27]>O>[C:3]1([C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=2)[CH:4]=[CH:5][CH:6]=[CH:7][C:2]=1[O:1][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][OH:27]

Komponenten

6

Edukt 4

HCID 5238Sodium IodideHCID 7017(1,1'-Biphenyl)-2-olHCID 14798Sodium HydroxideHCID 900121-Octanol, 8-chloro-

Produkt 1

HCID 66732740HCID 66732740, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

The compound was prepared using essentially the procedure of Preparatory Example 1 with 2-hydroxy biphenyl (40 g.), water (250 g.), sodium iodide (3.5 g.) and sodium hydroxide (37.6 g. of 50% in water). This mixture was heated to 100° C. with agitation and 8-chloro-1-octanol (77.4 g.) was added. The product was recovered essentially as in Preparatory Example 1.

Aufarbeitung

  1. customThe compound was prepared
  2. additionwas added
  3. customThe product was recovered essentially as in Preparatory Example 1

Quellen und Nachweise

ORD-Eintrag
ord-05054416c02248f89e5b132dca5599b6
Quelldatensatz
uspto-grants-2013_02
Patentnummer
US08378046B2

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