Sulfuric Acid → 6-Chlorohexanoic acid

Reaktionsgleichung

[C:1]([OH:8])(=[O:7])[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].S(=O)(=O)(O)O.[Cl:14]Cl>>[Cl:14][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][C:1]([OH:8])=[O:7]

Komponenten

Edukt 3

HCID 1118Sulfuric Acid

HCID 8892Hexanoic Acid

HCID 24526Chlorine

Produkt 1

HCID 202096-Chlorohexanoic acid

Versuchsvorschrift

147 parts by mass of the caproic acid were added to 1,000 parts by mass of 27N sulfuric acid saturated with chlorine and were reacted for 6 hours at 25° C. to obtain 95 parts by mass of 6-chlorocaproic acid.

Aufarbeitung

customwere reacted for 6 hours at 25° C.

Quellen und Nachweise

ORD-Eintrag: ord-f2882aa9cad04919ac8b08b0b5d0bd19
Quelldatensatz: uspto-grants-2003_05
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US06559275B2

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