Carbon Dioxide → HCID 178527662, Verbindung

HRID 414882Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 414882
C(=O)([O-])[O-].[Ag+2:5].[CH2:6]([S:11]([OH:14])(=[O:13])=[O:12])[S:7]([OH:10])(=[O:9])=[O:8].C(=O)=O>O>[CH2:6]([S:11]([O-:14])(=[O:13])=[O:12])[S:7]([O-:10])(=[O:9])=[O:8].[Ag+2:5]

Komponenten

5

Edukt 3

HCID 280Carbon DioxideHCID 10427Methanedisulfonic acidHCID 178418647HCID 178418647, Verbindung2×

Produkt 1

HCID 178527662HCID 178527662, VerbindungAusbeute 123,7 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

Silver carbonate (20 g, 0.0725 moles) was added to methanedisulfonic acid (25.55 g 50% solution in water) and diluted in 25 mL of distilled water while stirring. The silver carbonate dissolved with effervescence of carbon dioxide. After the reaction was complete, any remaining insoluble material was removed by filtration and the filtrate was stripped of water was removed under vacuum to give 25.3 g of pure silver methanedisulfonate.

Aufarbeitung

  1. customany remaining insoluble material was removed by filtration
  2. customwas removed under vacuum

Quellen und Nachweise

ORD-Eintrag
ord-7e11e4253b7d44f2a2c4ac9c3e72ef63
Quelldatensatz
uspto-grants-2012_01
Patentnummer
US08088548B2

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