Dimethyl Sulfide → Trimethylsulfonium Triflate
Reaktionsgleichung
[CH3:1][S:2][CH3:3].[CH3:4][O:5][S:6]([C:9]([F:12])([F:11])[F:10])(=[O:8])=[O:7]>ClCCl>[O-:8][S:6]([C:9]([F:12])([F:11])[F:10])(=[O:7])=[O:5].[CH3:1][S+:2]([CH3:4])[CH3:3]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
16 mmol of dimethyl sulfide was dissolved in 10 ml of dichloromethane at 0° C., and about 17 mmol of methyltrifluoromethane sulfonate was slowly dripped to the mixture to obtain a white solid product. The solid product was filtered and dried for 1 hour in an oven at 50° C. to obtain the following product:
Aufarbeitung
- customto obtain a white solid product
- filtrationThe solid product was filtered
- customdried for 1 hour in an oven at 50° C.
- customto obtain the following product
Quellen und Nachweise
- ORD-Eintrag
- ord-5cc9413dfef7447db1b13d03a866a5a8
- Quelldatensatz
- uspto-grants-2013_09
- Patentnummer
- US08536347B2
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