Santonox → N-(1-methylethyl)-3-(3-methoxyphenyl)-2-oxiranecarboxamide

HRID 435493

Reaktionsgleichung

Reaktionsgleichung von HRID 435493
[CH3:1][CH:2]([NH:4][C:5]([C:7](=O)C=CC1C=CC=C(OC)C=1)=[O:6])[CH3:3].Cl[C:20]1[CH:25]=[CH:24][CH:23]=[C:22]([C:26]([O:28]O)=O)[CH:21]=1.S(C1C(C)=CC(O)=C(C(C)(C)C)C=1)C1C(C)=C[C:34]([OH:41])=C(C(C)(C)C)C=1>C(Cl)CCl>[CH3:1][CH:2]([NH:4][C:5]([CH:7]1[CH:26]([C:22]2[CH:23]=[CH:24][CH:25]=[C:20]([O:41][CH3:34])[CH:21]=2)[O:28]1)=[O:6])[CH3:3]

Komponenten

5

Edukt 3

HCID 7308SantonoxHCID 70297m-Chloroperbenzoic acidHCID 54220101N-(1-methylethyl)-3-methoxycinnamoylcarboxamide

Produkt 1

HCID 20490547N-(1-methylethyl)-3-(3-methoxyphenyl)-2-oxiranecarboxamide

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 111,2-DichloroethaneLösungsmittel

Versuchsvorschrift

This compound was prepared from N-(1-methylethyl)-3-methoxycinnamoylcarboxamide (43.9 g.), m-chloroperbenzoic acid (46 g.), 4,4'-thiobis(6-tert-butyl-m-cresol) (0.6 g.), and ethylene dichloride (500 ml.) as described in Example 7. The compound obtained as an oil was used directly in the subsequent reaction.

Aufarbeitung

  1. customThe compound obtained as an oil
  2. customwas used directly in the subsequent reaction

Quellen und Nachweise

ORD-Eintrag
ord-944e9dd7c06e493285cdae4775af0b8b
Quelldatensatz
uspto-grants-1983_08
Patentnummer
US04401832

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