Diazomethane → 3'-Sulfamoyl-diazoacetophenone

HRID 461163

Reaktionsgleichung

Reaktionsgleichung von HRID 461163
[S:1]([C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][CH:13]=1)[C:8](Cl)=[O:9])(=[O:4])(=[O:3])[NH2:2].[N+:14](=[CH2:16])=[N-:15]>C(OCC)C>[S:1]([C:5]1[CH:6]=[C:7]([C:8](=[O:9])[CH:16]=[N+:14]=[N-:15])[CH:11]=[CH:12][CH:13]=1)(=[O:4])(=[O:3])[NH2:2]

Komponenten

4

Edukt 2

HCID 9550DiazomethaneHCID 188018833-Sulfamoylbenzoyl chloride

Produkt 1

HCID 537058143'-Sulfamoyl-diazoacetophenone

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 3283Diethyl EtherLösungsmittel

Versuchsvorschrift

11 g of 3-sulfamoylbenzoyl chloride were reacted as prescribed in Example 66b) with diazomethane in diethyl ether and the crystals were filtered off. Melting point: 142° C.

Aufarbeitung

  1. filtrationthe crystals were filtered off

Quellen und Nachweise

ORD-Eintrag
ord-29a7aeba45ad449fbac66113ff177cd3
Quelldatensatz
uspto-grants-1977_12
Patentnummer
US04061761

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