1,2-Dichloroethane → HCID 131716892, Verbindung

HRID 495960Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 495960
[CH2:1]([Cl:4])[CH2:2][Cl:3].[CH3:5][O:6][C:7](=[O:15])[C@H:8]([CH2:10][CH2:11][CH2:12][CH2:13][NH2:14])[NH2:9]>O>[CH2:1]([Cl:4])[CH2:2][Cl:3].[CH3:5][O:6][C:7](=[O:15])[C@H:8]([CH2:10][CH2:11][CH2:12][CH2:13][NH2:14])[NH2:9]

Komponenten

4

Edukt 2

HCID 111,2-Dichloroethane4×HCID 117779L-Lysine, methyl ester3×

Produkt 1

HCID 131716892HCID 131716892, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

A 0.4% (w/w) solution of HA in water was prepared. The pH of this solution was adjusted to between 4.3 and 4.75 by addition of acid. To each 100 ml of this solution was added 0.76 g of EDC with stirring until the EDC had completely dissolved. To each 100 ml of the HA/EDC solution was added 0.20 g of lysine methyl ester (LME) with stirring until the LME had completely dissolved. The addition of HA, EDC, and LME was conducted at room temperature; once the final HA/EDC/LME solution had been formed, it was stored at 4° C. until needed.

Aufarbeitung

  1. additionThe pH of this solution was adjusted to between 4.3 and 4.75 by addition of acid
  2. dissolutionhad completely dissolved
  3. dissolutionhad completely dissolved
  4. customwas conducted at room temperature

Quellen und Nachweise

ORD-Eintrag
ord-5a159504915f4894ad42a51bfd18ef87
Quelldatensatz
uspto-grants-2005_09
Patentnummer
US06943154B2

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