Acetic Acid → N-Benzylacetamide

HRID 538954

Reaktionsgleichung

Reaktionsgleichung von HRID 538954
[CH2:1]([NH2:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:9](O)(=[O:11])[CH3:10]>>[C:9]([NH:8][CH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1)(=[O:11])[CH3:10]

Komponenten

3

Edukt 2

HCID 176Acetic AcidHCID 7504Benzylamine

Produkt 1

HCID 11500N-Benzylacetamide

Reaktionsbedingungen

Temperatur
115 °C

Versuchsvorschrift

Benzylamine (1 mL) and acetic acid (20 mL) may be mixed together. The mixture may be heated at 115° C. for 17 hours. The excess acetic acid may be distilled from the reaction mixture using a rotary evaporator. The product may be crystallized from toluene. The mixture may be cooled to 0° C. and then filtered.

Aufarbeitung

  1. distillationThe excess acetic acid may be distilled from the reaction mixture
  2. customa rotary evaporator
  3. customThe product may be crystallized from toluene
  4. temperatureThe mixture may be cooled to 0° C.
  5. filtrationfiltered

Quellen und Nachweise

ORD-Eintrag
ord-27a2c44870504edb8d0db479262b468b
Quelldatensatz
uspto-grants-2014_10
Patentnummer
US08865920B2

Verknüpfte Notizen

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