Sulfur dichloride → 2-(Cyclohexyloxy)acetyl chloride
Reaktionsgleichung
[CH:1]1([O:7][CH2:8][C:9]([OH:11])=O)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[Cl:12]SCl>>[CH:1]1([O:7][CH2:8][C:9]([Cl:12])=[O:11])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1Komponenten
3
Versuchsvorschrift
A mixture of 2-(cyclohexyloxy)acetic acid (0.90 g, 5.69 mmol) and dichlorosulfane (10 mL) was refluxed for 2 h. The mixture was cooled to rt and concentrated in vacuo to give the title compound as yellow oil, which was used for next step without further purification.
Aufarbeitung
- temperaturewas refluxed for 2 h
- concentrationconcentrated in vacuo
Quellen und Nachweise
- ORD-Eintrag
- ord-8af8cc706d3a457badbaab90d0f5f777
- Quelldatensatz
- uspto-grants-2016_09
- Patentnummer
- US09434695B2
Notizen zur Reaktion
Wird geladen…