Sulfur dichloride → 2-(Cyclohexyloxy)acetyl chloride

HRID 56266

Reaktionsgleichung

Reaktionsgleichung von HRID 56266
[CH:1]1([O:7][CH2:8][C:9]([OH:11])=O)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[Cl:12]SCl>>[CH:1]1([O:7][CH2:8][C:9]([Cl:12])=[O:11])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Komponenten

3

Edukt 2

HCID 25353Sulfur dichlorideHCID 191994Cyclohexoxyacetic acid

Produkt 1

HCID 124841232-(Cyclohexyloxy)acetyl chloride

Versuchsvorschrift

A mixture of 2-(cyclohexyloxy)acetic acid (0.90 g, 5.69 mmol) and dichlorosulfane (10 mL) was refluxed for 2 h. The mixture was cooled to rt and concentrated in vacuo to give the title compound as yellow oil, which was used for next step without further purification.

Aufarbeitung

  1. temperaturewas refluxed for 2 h
  2. concentrationconcentrated in vacuo

Quellen und Nachweise

ORD-Eintrag
ord-8af8cc706d3a457badbaab90d0f5f777
Quelldatensatz
uspto-grants-2016_09
Patentnummer
US09434695B2

Verknüpfte Notizen

Wird geladen…