Water → Phenol

HRID 631759

Reaktionsgleichung

Reaktionsgleichung von HRID 631759
[CH:1]1([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[OH2:13]>>[C:1]1(=[O:13])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[C:1]1([OH:13])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:7][CH:12]1[CH2:8][CH2:9][CH2:10][C:11]1=[O:13]

Komponenten

5

Edukt 2

HCID 962WaterHCID 13229Cyclohexylbenzene

Produkt 3

HCID 996PhenolHCID 7967CyclohexanoneHCID 142652-Methylcyclopentanone

Versuchsvorschrift

The neutralized cleavage reaction product mixture can then be separated by methods such as distillation. In one example, in a first fractionation column after the cleavage reactor, a heavies fraction comprising the amine salt is obtained at the bottom of the column, a side fraction comprising cyclohexylbenzene is obtained in the middle section, and an upper fraction comprising cyclohexanone, phenol, methylcyclopentanone, and water is obtained.

Aufarbeitung

  1. customThe neutralized cleavage reaction product mixture can then be separated by methods such as distillation
  2. customis obtained at the bottom of the column
  3. customis obtained in the middle section

Quellen und Nachweise

ORD-Eintrag
ord-ca2a3698fec944b89e120b7f0aeaca5d
Quelldatensatz
uspto-grants-2016_04
Patentnummer
US09321711B2

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