Dipotassium tetrachloroplatinate → Platinous chloride

HRID 653083

Reaktionsgleichung

Reaktionsgleichung von HRID 653083
Cl.Cl.[C:3]1([CH2:9][NH2:10])([CH2:7][NH2:8])[CH2:6][CH2:5][CH2:4]1.C([O-])(=O)C.[Na+].[Cl:16][Pt-2:17](Cl)(Cl)[Cl:18].[K+].[K+]>O>[C:3]1([CH2:9][NH2:10])([CH2:7][NH2:8])[CH2:6][CH2:5][CH2:4]1.[Pt:17]([Cl:18])[Cl:16]

Komponenten

6

Edukt 3

HCID 61440Dipotassium tetrachloroplatinateHCID 517045Sodium AcetateHCID 202036281,1-Bis(aminomethyl)cyclobutane dihydrochloride

Produkt 2

HCID 2770Platinous chlorideHCID 4328361,1-Cyclobutanedimethanamine

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

A solution of 1.87 g of the above amine in 30 ml of water was treated with 1.64 g of solid sodium acetate followed by 4.15 g of potassium tetrachloroplatinate. The mixture was stirred overnight and filtered. The filtrate was concentrated, giving as a solid 1,1-cyclobutanedimethanamine, compound with platinum chloride.

Aufarbeitung

  1. filtrationfiltered
  2. concentrationThe filtrate was concentrated

Quellen und Nachweise

ORD-Eintrag
ord-e8ec9817642b46d08a31487737b3a61d
Quelldatensatz
uspto-grants-1987_06
Patentnummer
US04675336

Verknüpfte Notizen

Wird geladen…