Malonic acid, disodium salt → Zinc Malonate Dihydrate

HRID 733500

Reaktionsgleichung

Reaktionsgleichung von HRID 733500
O.O.N[C@H](C([O-])=O)CCC([O-])=[O:8].[Zn+2:13].C([O-])(=O)CC([O-])=[O:17].[Na+].[Na+].[CH2:23]([C:27]([O-:29])=[O:28])[C:24]([O-:26])=[O:25].[Cl-].[Zn+2].[Cl-]>O>[OH2:8].[OH2:17].[C:27]([O-:29])(=[O:28])[CH2:23][C:24]([O-:26])=[O:25].[Zn+2:13]

Komponenten

6

Edukt 4

HCID 8865Malonic acid, disodium saltHCID 9084Malonate IonHCID 3007855ZincchlorideHCID 22825209Zinc L-glutamate Dihydrate

Produkt 1

HCID 86616729Zinc Malonate Dihydrate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

Basically the reaction conditions found for preparation of zinc L-glutamate (Example 13) was employed. A suspension of sodium malonate (white coloured) is prepared by adding 100 mL of millipore water to 16.605 g (0.1 moles) of solid sodium malonate dibasic monohydrate (SIGMA M1875-100G, MW 166.05, CAS 26522-85-0) in a 250 mL beaker. To this suspension was added 13.628 g (0.1 moles) of solid zinc chloride (FLUKA, 96469, MW 136.3, CAS 7646-85-7). Subsequent manufacturing steps were as described in Example 13.

Aufarbeitung

  1. customBasically the reaction conditions
  2. customis prepared

Quellen und Nachweise

ORD-Eintrag
ord-61926276b95f4951b769df7926e9ab35
Quelldatensatz
uspto-grants-2009_09
Patentnummer
US07589235B2

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