Sucrose → Divinylbenzene Methacrylic Acid

HRID 734162

Reaktionsgleichung

O[CH2:2][C@H:3]([C@@H:5]([C@H:7]([C@H](CO)O)O)O)O.[CH2:13](O)[C@H]1O[C@H](O[C@:21]2([CH2:30]O)O[C@H:24]([CH2:26]O)[C@@H:23](O)[C@@H:22]2O)[C@H](O)[C@@H](O)[C@@H]1O.C(O)[C@H]1[O:43][C:41](=[O:42])[C@H:40](O)[C@@H:39](O)[C@@H]1O>>[CH:5]([C:3]1[CH:2]=[CH:26][CH:24]=[CH:23][C:22]=1[CH:21]=[CH2:30])=[CH2:7].[C:41]([OH:43])(=[O:42])[C:40]([CH3:13])=[CH2:39]

Komponenten

Edukt 3

HCID 5988Sucrose

HCID 7027delta-Gluconolactone

HCID 82170L-Sorbitol

Produkt 1

HCID 66647846Divinylbenzene Methacrylic Acid

Versuchsvorschrift

Ingredients. (1) Diglycerol 10.0 (2) Sucrose 74.0 (3) Gluconolactone (10% solution in water) 10.0 (4) Preservative 1.0 (5) Divinylbenzene/methacrylic acid copolymer 1.0 (6) Zeolite 4.0. Procedure. Mix (2) to (5) and heat at 90 to 120 C. for 30 to 45 minutes to a clear liquid. Add (1) and (6) and mix. Cool to room temperature. An opaque mobile sticky liquid is obtained.

Aufarbeitung

temperatureheat at 90 to 120 C
additionmix
customAn opaque mobile sticky liquid is obtained

Quellen und Nachweise

ORD-Eintrag: ord-9cc4c8921e6e4e4da953694505dfc186
Quelldatensatz: uspto-grants-2009_09
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US07592002B2

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