2-(6-Methoxy-2-naphthyl)propionic acid → HCID 178487451, Verbindung

Reaktionsgleichung

NCc1ccc(F)cc1F.COc1ccc2cc(C(C)C(=O)O)ccc2c1.C1=CC=C(C=C1)P(=O)(C2=CC=CC=C2)Cl.CCN(C(C)C)C(C)C.CN(C)C=O>>COc1ccc2cc(C(C)C(=O)NCc3ccc(F)cc3F)ccc2c1

addition150 uL of MeCN/H2O (1:1) mixed solvent was dispensed separately into each plate using the 96-tip head of the Tecan Evo-200.
addition150 uL of internal standard solution was dispensed separately into each plate using the 96-tip head of the Tecan Evo-200.
aliquot10 uL aliquot taken from reaction vials, and added to pre-filled wells in the transfer plate.
addition380 uL MeCN solvent were added to the transfer plate
aliquot20 uL taken from transfer plate to filter plate 1 for LCMS analysis
addition180 uL MeCN added to filter plate 1 for LCMS analysis
aliquot10 uL taken from transfer plate to filter plate 2 for TOF-DESI analysis
addition190 uL MeCN added to filter plate 2 for TOF-DESI analysis
customthe 96-well filter plates were centrifuged for 2.5 min at 3000 RPM

Wird geladen…

addition150 uL of MeCN/H2O (1:1) mixed solvent was dispensed separately into each plate using the 96-tip head of the Tecan Evo-200.
addition150 uL of internal standard solution was dispensed separately into each plate using the 96-tip head of the Tecan Evo-200.
aliquot10 uL aliquot taken from reaction vials, and added to pre-filled wells in the transfer plate.
addition380 uL MeCN solvent were added to the transfer plate
aliquot20 uL taken from transfer plate to filter plate 1 for LCMS analysis
addition180 uL MeCN added to filter plate 1 for LCMS analysis
aliquot10 uL taken from transfer plate to filter plate 2 for TOF-DESI analysis
addition190 uL MeCN added to filter plate 2 for TOF-DESI analysis
customthe 96-well filter plates were centrifuged for 2.5 min at 3000 RPM

Wird geladen…