Trifluoroacetic acid → HCID 178508837, Verbindung

HRID 905504

Reaktionsgleichung

Reaktionsgleichung von HRID 905504
[NH2:1][C:2]1[N:6]=[C:5]([NH2:7])[NH:4][N:3]=1.[F:8][C:9]([F:14])([F:13])[C:10]([OH:12])=[O:11]>O>[O-:12][C:10]([C:9]([F:14])([F:13])[F:8])=[O:11].[NH2:1][C:2]1[NH:3][NH+:4]=[C:5]([NH2:7])[N:6]=1

Komponenten

4

Edukt 2

HCID 6422Trifluoroacetic acidHCID 150783,5-Diamino-1,2,4-triazole

Produkt 1

HCID 178508837HCID 178508837, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

3,5-Diamino-1,2,4-triazole (1.50 g, 15.14 mmol) was dissolved in 5 ml of distilled water. Trifluoroacetic acid (1.12 ml, 15.14 mmol) was added via syringe at room temperature and the reaction was stirred at room temperature for 1 hour. The water was removed in vacuo with heating to approximately 90° C. for 4 hours.

Aufarbeitung

  1. customThe water was removed in vacuo
  2. temperaturewith heating to approximately 90° C. for 4 hours

Quellen und Nachweise

ORD-Eintrag
ord-e08f5efc7a6e4caaaed595895ce16a64
Quelldatensatz
uspto-grants-2011_09
Patentnummer
US08012277B2

Verknüpfte Notizen

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