Carbon Dioxide → HCID 178514403, Verbindung

HRID 905513

Reaktionsgleichung

Reaktionsgleichung von HRID 905513
[N:1]([CH2:10][C:11]([OH:13])=[O:12])([CH2:6][C:7]([OH:9])=[O:8])[CH2:2][C:3]([OH:5])=[O:4].C(=O)(O)O.[NH2:18][NH:19][C:20]([NH2:22])=[NH:21].C(=O)=O>O>[N:1]([CH2:2][C:3]([O-:5])=[O:4])([CH2:6][C:7]([O-:9])=[O:8])[CH2:10][C:11]([O-:13])=[O:12].[NH2:18][NH:19][C:20]([NH2:22])=[NH2+:21].[NH2:18][NH:19][C:20]([NH2:22])=[NH2+:21].[NH2:18][NH:19][C:20]([NH2:22])=[NH2+:21]

Komponenten

5

Edukt 3

HCID 280Carbon DioxideHCID 8758Nitrilotriacetic AcidHCID 178513185HCID 178513185, Verbindung

Produkt 1

HCID 178514403HCID 178514403, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

Nitrilotriacetic acid (1.0 g, 5.23 mmol) was dissolved in 10 ml of distilled water. Aminoguanidine bicarbonate (2.14 g, 15.69 mmol) was added in portions at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for three days. The water was removed in vacuo with heating to approximately 90° C. The product was isolated as a white solid.

Aufarbeitung

  1. customThe water was removed in vacuo
  2. temperaturewith heating to approximately 90° C
  3. customThe product was isolated as a white solid

Quellen und Nachweise

ORD-Eintrag
ord-3a1b04a135ae49119311cf305d8c8721
Quelldatensatz
uspto-grants-2011_09
Patentnummer
US08012277B2

Verknüpfte Notizen

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