Sulfuric Acid → Prop-2-enamide;trimethyl(2-prop-2-enoyloxyethyl)azanium;chloride

HRID 963595

Reaktionsgleichung

Reaktionsgleichung von HRID 963595
COC(C1SC=CC=1S(NCC1C=CC2OCOC=2C=1)(=O)=O)=O.S(=O)(=O)(O)O.[C:29]([NH2:33])(=[O:32])[CH:30]=[CH2:31].[Cl-:34].[C:35]([O:39][CH2:40][CH2:41][N+:42]([CH3:45])([CH3:44])[CH3:43])(=[O:38])[CH:36]=[CH2:37].Br([O-])(=O)=O.[Na+].[Na+].[Na+].[Na+].[Na+].C(N(CC([O-])=O)CC([O-])=O)CN(CC([O-])=O)CC([O-])=O>O>[Cl-:34].[C:35]([O:39][CH2:40][CH2:41][N+:42]([CH3:44])([CH3:43])[CH3:45])(=[O:38])[CH:36]=[CH2:37].[C:29]([NH2:33])(=[O:32])[CH:30]=[CH2:31]

Komponenten

8

Edukt 6

HCID 1118Sulfuric AcidHCID 6144Edetate SodiumHCID 6579AcrylamideHCID 162071Ethanaminium, N,N,N-trimethyl-2-[(1-oxo-2-propen-1-yl)oxy]-, chloride (1:1)HCID 3476271Methyl 3-(1,3-benzodioxol-5-ylmethylsulfamoyl)thiophene-2-carboxylateHCID 23668195Sodium Bromate

Produkt 1

HCID 155211Prop-2-enamide;trimethyl(2-prop-2-enoyloxyethyl)azanium;chloride

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

An organic solution is prepared by combining a low odor paraffin oil (208.4 g), polyoxyethylene sorbitan monooleate (9.0 g) and polyoxyethylene sorbitan trioleate (32.6 g) in a reactor with stirring. To this solution is added an aqueous solution, adjusted to pH=3.5 with sulfuric acid, containing acrylamide (24.0 g), acryloxyethyltrimethyl ammonium chloride (80.2 g), sodium bromate (0.01 g), ethylenediaminetetraacetic acid tetra sodium salt (0.21 g), and water (145.58 g).

Aufarbeitung

  1. customAn organic solution is prepared
  2. additionTo this solution is added an aqueous solution

Quellen und Nachweise

ORD-Eintrag
ord-41ad4684ef184b0cbe581df66839c52f
Quelldatensatz
uspto-grants-1998_06
Patentnummer
US05763530

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