Methylmalonic Acid → HCID 14073324, Verbindung

HRID 973782

Reaktionsgleichung

Reaktionsgleichung von HRID 973782
[CH3:1][CH:2]([C:6](O)=O)[C:3]([OH:5])=[O:4].[CH3:9][NH:10][CH3:11].C=O>O>[CH3:9][N:10]([CH3:11])[CH2:6][CH:2]([CH3:1])[C:3]([OH:5])=[O:4]

Komponenten

5

Edukt 3

HCID 487Methylmalonic AcidHCID 674DimethylamineHCID 712Formaldehyde

Produkt 1

HCID 14073324HCID 14073324, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Reaktionsbedingungen

Temperatur
0 °C

Versuchsvorschrift

In 1.0 ml of water was dissolved 1.5 g of methylmalonic acid, after which 1.26 g of a 50% aqueous dimethylamine solution and 0.96 ml of a 37% aqueous formaldehyde solution were added with stirring at 0° C., and the resulting mixture was stirred at 0° to 5° C. for 3 hours and then at 80° C. for 30 minutes.

Aufarbeitung

  1. stirringthe resulting mixture was stirred at 0° to 5° C. for 3 hours

Quellen und Nachweise

ORD-Eintrag
ord-cc3d7a87fd854185b231c67ec2bf855a
Quelldatensatz
uspto-grants-1991_11
Patentnummer
US05064945

Verknüpfte Notizen

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