[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][N:3]=1.[N+:8]([CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][N+:16]#[C-:17])#[C-:9].[CH:18](=O)[C:19]1[O:23][CH:22]=[CH:21][CH:20]=1>Cl(O)(=O)(=O)=O>[O:23]1[CH:22]=[CH:21][CH:20]=[C:19]1[C:18]1[N:1]=[C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][N:3]2[C:9]=1[NH:8][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][N+:16]#[C-:17]Compound (2) was prepared in accordance with general instructions 1 from 1.0 ml 2-aminopyridine solution (0.1 M, MC), 0.575 ml 1,6-diisocyanohexane solution (0.2 M, MC), 0.500 ml furfural solution (0.3 M, MC), and 10 μl perchloric acid (w=20%).
Wird geladen…