Fluorobenzene → Ethylene carbonate

HRID 1010505

Reaction equation

HRID 1010505 reaction equation
[C:1]1(=[O:6])[O:5][CH:4]=[CH:3][O:2]1.[C:7]1(=[O:14])[O:11][CH2:10][CH:9]([CH:12]=C)[O:8]1.FC1C=CC=CC=1>>[C:1]1(=[O:6])[O:5][CH2:4][CH2:3][O:2]1.[C:7](=[O:14])([O:8][CH2:9][CH3:12])[O:11][CH3:10]

Participants

5

Reactant 3

HCID 10008FluorobenzeneHCID 13385Vinylene carbonateHCID 27350381,3-Dioxolan-2-one, 4-ethenyl-

Product 2

HCID 7303Ethylene carbonateHCID 522046Ethyl methyl carbonate

Procedure

A mixed solvent of ethylene carbonate and methyl ethyl carbonate was prepared at a capacity ratio of 10:30. To the mixed solvent, 2% by weight of vinylene carbonate, 2% by weight of vinylethylene carbonate, 5% by weight of fluorobenzene, and 5% by weight of phosphazene were added, obtaining a mixed solution. LiPF6 was dissolved in this mixed solution at a concentration of 1.5 mol/L, obtaining a non-aqueous electrolyte.

Workup

  1. customobtaining a mixed solution
  2. customobtaining a non-aqueous electrolyte

Sources & evidence

ORD record
ord-9ec6975ef85a4f62816cb052ea0f97de
Source dataset
uspto-grants-2011_07
Patent number
US07976983B2

Linked notes

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