Sucrose → HCID 69927845, compound

HRID 1076820Notes

Reaction equation

HRID 1076820 reaction equation
[CH2:1]([OH:23])[C@H:2]1[O:7][C@@H:6]([O:8][C@H:9]2[C@H:13]([OH:14])[C@@:12]([OH:17])([CH2:15][OH:16])[O:11][C@@H:10]2[CH2:18][OH:19])[C@H:5]([OH:20])[C@@H:4]([OH:21])[C@H:3]1[OH:22].[CH2:24]([OH:46])[C@H:25]1[O:30][C@H:29]([O:31][C@:32]2([CH2:41][OH:42])[O:36][C@H:35]([CH2:37][OH:38])[C@@H:34]([OH:39])[C@@H:33]2[OH:40])[C@H:28]([OH:43])[C@@H:27]([OH:44])[C@@H:26]1[OH:45]>>[CH2:24]([OH:46])[C@H:25]1[O:30][C@H:29]([O:31][C@:32]2([CH2:41][OH:42])[O:36][C@H:35]([CH2:37][OH:38])[C@@H:34]([OH:39])[C@@H:33]2[OH:40])[C@H:28]([OH:43])[C@@H:27]([OH:44])[C@@H:26]1[OH:45].[CH2:1]([OH:23])[C@H:2]1[O:7][C@@H:6]([O:8][C@H:9]2[C@H:13]([OH:14])[C@@:12]([OH:17])([CH2:15][OH:16])[O:11][C@@H:10]2[CH2:18][OH:19])[C@H:5]([OH:20])[C@@H:4]([OH:21])[C@H:3]1[OH:22]

Participants

3

Reactant 2

HCID 5988SucroseHCID 11333Lactulose

Product 1

HCID 69927845HCID 69927845, compound

Procedure

A mixture of lactitol in fine powder, from 100 to 50 mesh, and air, in a mixing ratio of 10-20%, v/v, is injected from the center nozzle of a two-fluid nozzle attached on the top of a spray-drying tower. Separately, a 75% aqueous sucrose solution which is cooled gradually with agitation and which is beginning to crystallize is sprayed through the outer nozzle applying a pressure of 50 to 100 kg/cm2 to allow the sprayed solution to contact with powderd lactitol and then the mixture is dried with hot air charged from the top of the drying tower. Alternatively, a sucrose solution as described above may be sprayed on a horizontal fluidized-bed of lactitol fine powder, and the lactitol powder and the sucrose drops may be dried as a whole to obtain a crystalline sucrose-lactitol product. The mixing ratio of sucrose and lactitol is adjusted to meet the degree required for the product as table sugar.

Workup

  1. customto crystallize
  2. customthe mixture is dried with hot air
  3. additioncharged from the top of the drying tower
  4. dry with materialthe lactitol powder and the sucrose drops may be dried as a whole

Sources & evidence

ORD record
ord-358285e0a44d44b999644764a1a6613a
Source dataset
uspto-grants-1976_05
Patent number
US03957976

Reaction notes

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