Reaction equation
[C:1]1([CH:7]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[C:8](Cl)=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:17][CH:18]([CH3:22])[CH2:19][CH2:20][NH2:21]>>[CH3:17][CH:18]([CH3:22])[CH2:19][CH2:20][NH:21][C:8](=[O:9])[CH:7]([C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)[C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1Participants
3
Procedure
The title compound, white solid, m.p. 128° C. and MS: m/e=281 (M+) was prepared in accordance with the general method of example 1 from diphenylacetyl chloride and 3-methyl-butylamine.
Sources & evidence
- ORD record
- ord-ef388296f2014e0ebbe2b7839553ca40
- Source dataset
- uspto-grants-2003_04
- Patent number
- US06548522B1
Linked notes
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