Ammonium Acetate → 5,6,7,8-Tetrahydroquinolin-7-amine
Reaction equation
C([O-])(=O)C.[NH4+:5].[N:6]1[C:15]2[CH:14]=[CH:13][CH2:12][CH2:11][C:10]=2[CH:9]=[CH:8][CH:7]=1>C(OCC)(=O)C>[NH2:5][CH:13]1[CH2:14][C:15]2[N:6]=[CH:7][CH:8]=[CH:9][C:10]=2[CH2:11][CH2:12]1Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
This compound was prepared from ammonium acetate (1 54 g, 20 mmol) and 5,6-dihydroquinoline (2.31 g, 10 mmol) using the method described in Example 36 and ethyl acetate instead of ether as the extracting solvent.
Sources & evidence
- ORD record
- ord-bdf9e9eabb9b4bea854547bbdd2e0ff7
- Source dataset
- uspto-grants-1991_12
- Patent number
- US05075303
Reaction notes
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