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3-fluoro-N,N-dimethylbenzenesulfonamide → HCID 130058621, compound

HRID 1490679
Notes
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Reaction equation

HRID 1490679 reaction equation
CN(C)S(=O)(=O)c1cccc(F)c1>C1CCOC1.CC(C)(C)C(=O)[O][Co][O]C(=O)C(C)(C)C.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.Cc1cc(CP(C(C)C)C(C)C)nc(CP(C(C)C)C(C)C)c1>CN(C)S(=O)(=O)c1ccc(B2OC(C)(C)C(C)(C)O2)c(F)c1
ParticipantsConditionsSources & evidenceReaction notes

Participants

5

Reactant 1

HCID 606398363-fluoro-N,N-dimethylbenzenesulfonamide

Product 1

HCID 130058621HCID 130058621, compoundYield 98%

Reagents, catalysts & solvents 3

HCID 2733548Bis(pinacolato)diboraneReagentHCID 178447600HCID 178447600, compoundCatalystHCID 8028TetrahydrofuranSolvent

Conditions

Temperature
80 °C

Sources & evidence

ORD record
ord-857a66351a344631929443ecb6ee5e50
Source dataset
Borylation dataset from Roche
DOI
10.1021/jacs.6b13346

Reaction notes

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On this pageParticipantsConditionsSources & evidenceReaction notes