Aniline → HCID 178425477, compound
Reaction equation
[H-].[Na+:2].NC1C=CC=CC=1.[CH3:10][C:11]1[C:12]([CH3:17])=[C:13]([CH3:16])[CH2:14][CH:15]=1>O1CCCC1>[CH3:10][C:11]1[CH:15]=[CH:14][C:13]([CH3:16])([Na:2])[C:12]=1[CH3:17]Participants
5
Reactant 3
Product 1
Reagents, catalysts & solvents 1
Conditions
- Temperature
- 50 °C
Procedure
Sodium hydride (containing mineral oil; the content of sodium hydride: 60%) (0.80 g) and aniline (0.046 g) were added to the solution of trimethylcyclopentadiene (1.08 g) dissolved in tetrahydrofuran (6.12 g), and stirred at 50° C. for 3 hours. Thus, trimethylcyclopentadienylsodium was obtained in the form of a solution in tetrahydrofuran.
Sources & evidence
- ORD record
- ord-be34fdff6d8d4ce9a642a171482e678f
- Source dataset
- uspto-grants-2001_03
- Patent number
- US06197990B1
Reaction notes
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