Hydroquinone → Dicumyl peroxide

HRID 1601477

Reaction equation

HRID 1601477 reaction equation
C[O-].[Na+].[O-2].[Al+3].[O-2].[O-2].[Al+3].[C:9]1([CH:16]=[CH:15][C:13](O)=[CH:12][CH:11]=1)O.C[CH2:18][C:19]([O:23][O:24][C:25](OO)([CH2:27]C)[CH3:26])(OO)[CH3:20].CN(C)[C:33]1[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=1>ClCCl.C1(C)C=CC=CC=1>[C:19]([O:23][O:24][C:25]([C:33]1[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=1)([CH3:27])[CH3:26])([C:9]1[CH:16]=[CH:15][CH:13]=[CH:12][CH:11]=1)([CH3:20])[CH3:18]

Participants

8

Reactant 5

HCID 785HydroquinoneHCID 949N,N-DimethylanilineHCID 3672772Methyl ethyl ketone peroxideHCID 9989226AluminaHCID 10942334Sodium Methoxide

Product 1

HCID 6641Dicumyl peroxide

Reagents, catalysts & solvents 2

HCID 1140TolueneSolventHCID 6344DichloromethaneSolvent

Procedure

Sodium methoxide (NaOCH3), toluene (anhydrous), dichloromethane, hexanes, activated neutral aluminum oxide (60 to 50 mesh), hydroquinone, methyl ehtyl ketone peroxide, dimethylaniline, dicumylperoxide were obtained from commercial sources and used as received.

Sources & evidence

ORD record
ord-c184df2281e94453b3f0a43f9683210f
Source dataset
uspto-grants-1999_11
Patent number
US05977269

Linked notes

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