Reaction equation
C1CCNCC1.O=C1Nc2ccc(Cl)cc2[C@@](C#CC2CC2)(C(F)(F)F)O1>C1CN2CCN1CC2.COCCOC.CS(C)=O.O=C1OC2(c3ccc(O)cc3Oc3cc(O)ccc32)c2ccccc21.[Cl][Ni][Cl]>O=C1Nc2ccc(N3CCCCC3)cc2C(C#CC2CC2)(C(F)(F)F)O1Participants
7
Conditions
- Temperature
- 55 °C
Workup
- additionThe samples was moved from a 1536 well plate into a 384 well plate. The 384 well plate contained 75 microliter of 1% Acetic acid in DMSO solution with 0.003M trimethoxybenzene. The reaction plate was rinsed three times with the same solution to make a total addition volume of ~90 microliters
- aliquot25 microliter of quenched reaction mixture was taken
- additionTo the 25 microliter aliquot 50 microliter of DMSO was added. If the original reaction concentration was 0.05 M (wrt limiting reagent). This would make a final analytical concentration of 0.36 mM which is in line with typical analytical concentrations from this group.
Sources & evidence
- ORD record
- ord-5d1b49fbfb694abf91120dc2b28bd4f8
- Source dataset
- Nano CN PhotoChemistry Informers Library
- Original link
- View source
Linked notes
Loading…