3-Chloropyridine → HCID 44243553, compound
Reaction equation
Cc1noc(C)c1B1OC(C)(C)C(C)(C)O1.Clc1cccnc1>C1CCC2=NCCCN2CC1.C1CCOC1.CS(=O)(=O)[O][Pd][c]1ccccc1-c1ccccc1N.O.c1ccc(P(c2ccccc2)c2ccccc2)cc1>Cc1noc(C)c1-c1cccnc1Participants
10
Reactant 2
Product 1
Reagents, catalysts & solvents 7
Conditions
- Temperature
- 110 °C
Workup
- additionAs soon as the slug leaves the reactor and is detected at PS2,a quench solution volume equal to the reaction slug volume(prepared slug volume + base injection volume) is injected into the reaction slug
Sources & evidence
- ORD record
- ord-b47ff896ca034a5dbf6308a6b8f8bd3a
- Source dataset
- Reizman Suzuki Cross-Coupling
- Original link
- View source
Reaction notes
Loading…