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Putrescine → Dodecane

HRID 1833331
Notes
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Reaction equation

HRID 1833331 reaction equation
C(C1C=C(CCC(NCCCCNC(=O)CCC2C=C(C(C)(C)C)C(O)=C(C(C)(C)C)C=2)=O)C=C(C(C)(C)C)C=1O)(C)(C)C.C(C1C=C(CCC(NCCCCCCCCNC(=O)CCC2C=C(C(C)(C)C)C(O)=C(C(C)(C)C)C=2)=O)C=C(C(C)(C)C)C=1O)(C)(C)C.C(C1C=C(CCC(Cl)=O)C=C(C(C)(C)C)C=1O)(C)(C)C.NCCCCN.NCCCCCCCCN.N[CH2:130][CH2:131][CH2:132][CH2:133][CH2:134][CH2:135][CH2:136][CH2:137][CH2:138][CH2:139][CH2:140][CH2:141]N>>[CH3:141][CH2:140][CH2:139][CH2:138][CH2:137][CH2:136][CH2:135][CH2:134][CH2:133][CH2:132][CH2:131][CH3:130]
ParticipantsProcedureSources & evidenceReaction notes

Participants

7

Reactant 6

HCID 1045PutrescineHCID 177271,12-DodecanediamineHCID 242501,8-OctanediamineHCID 148576471,4-Bis[beta-(3,5-di-t-butyl-4-hydroxy phenyl) propionamido] butaneHCID 156069683-(3,5-Di-tert-butyl-4-hydroxyphenyl)propionyl chlorideHCID 23337168
1,8-Bis[beta-(3,5-di-t-butyl-4-hydroxy phenyl) propionamido] octane

Product 1

HCID 8182Dodecane

Procedure

Using techniques similar to the one described above 1,4-bis[β-(3,5-di-t-butyl-4-hydroxy phenyl) propionamido] butane (M.P. 203°-205° C); 1,8-bis[β-(3,5-di-t-butyl-4-hydroxy phenyl) propionamido] octane (M.P. 94.5°-96° C); and 1,12-bis[β-3,5-di-t-butyl-4-hydroxy phenyl) propionamido] dodecane (M.P. 89°-92° C) were prepared by reaction of β-(3,5-di-t-butyl-4-hydroxy phenyl) propionyl chloride with respectively 1,4 diamino butane, 1,8-diamino octane and 1,12-diamino dodecane.

Sources & evidence

ORD record
ord-8ed7d1089d1642dea35085cad8314e99
Source dataset
uspto-grants-1978_01
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US04066610

Reaction notes

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On this pageParticipantsProcedureSources & evidenceReaction notes