Hydrochloric Acid → Triethanolamine hydrochloride

HRID 2165793Notes

Reaction equation

HRID 2165793 reaction equation
[N:1]([CH2:8][CH2:9][OH:10])([CH2:5][CH2:6][OH:7])[CH2:2][CH2:3][OH:4].[ClH:11]>O>[ClH:11].[N:1]([CH2:8][CH2:9][OH:10])([CH2:5][CH2:6][OH:7])[CH2:2][CH2:3][OH:4]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 7618Triethanolamine

Product 1

HCID 101814Triethanolamine hydrochloride

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

100 parts of triethanolamine were dissolved in 500 parts of water. 100 parts of concentrated hydrochloric acid were added to the solution to give a triethanolamine hydrochloride solution. This solution was added dropwise to a solution of 50 parts of C. I. Solubilized Sulphur Black 1 in 500 parts of boiling water under stirring. A crystallization began immediately. The crystal thus formed was separated by filtration, washed with water and dried to give a water-insoluble black pigment of the following formula:

Sources & evidence

ORD record
ord-a0331ee03407497d92ad0b812a8e2ff0
Source dataset
uspto-grants-1990_07
Patent number
US04941923

Reaction notes

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