Acetaldehyde → HCID 69731780, compound

HRID 22809

Reaction equation

HRID 22809 reaction equation
[NH2:1][C:2]1[C:7]([O:8][CH2:9][C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)=[CH:6][CH:5]=[CH:4][N:3]=1.[N+:16]([CH2:18][C:19]([O:21][CH3:22])=[O:20])#[C-:17].[CH:23](=O)[CH3:24]>Cl(O)(=O)(=O)=O>[CH3:22][O:21][C:19](=[O:20])[CH2:18][NH:16][C:17]1[N:3]2[CH:4]=[CH:5][CH:6]=[C:7]([O:8][CH2:9][C:10]3[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=3)[C:2]2=[N:1][C:23]=1[CH3:24]

Participants

5

Reactant 3

HCID 177AcetaldehydeHCID 903342-Amino-3-benzyloxypyridineHCID 547815Methyl isocyanoacetate

Product 1

HCID 69731780HCID 69731780, compound

Reagents, catalysts & solvents 1

HCID 24247Perchloric AcidSolvent

Procedure

Compound (31) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-3-benzyloxypyridine solution (0.1 M, DCM), 0.575 ml of methyl isocyanoacetate solution (0.2 M, DCM), 0.500 ml of acetaldehyde solution (0.3 M, DCM), and 10 μl of perchloric acid (w=20%).

Sources & evidence

ORD record
ord-cf3f0544354a4906b653eb322f8d020a
Source dataset
uspto-grants-2005_02
Patent number
US06849642B2

Linked notes

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