Dimethylformamide dimethyl acetal → HCID 54199707, compound
Reaction equation
[CH3:1][C:2]1[C:7]([C:8]([C:10]2[C:19]3[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=3)[CH:13]=[CH:12][CH:11]=2)=[O:9])=[CH:6][CH:5]=[CH:4][C:3]=1[N+:20]([O-:22])=[O:21].[CH3:23][N:24]([CH:26](OC)OC)[CH3:25]>CN(C=O)C>[CH3:23][N:24]([CH3:26])[CH:25]=[CH:1][C:2]1[C:7]([C:8]([C:10]2[C:19]3[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=3)[CH:13]=[CH:12][CH:11]=2)=[O:9])=[CH:6][CH:5]=[CH:4][C:3]=1[N+:20]([O-:22])=[O:21]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
Following a procedure similar to that described in Preparation 2A above, 57 g (0.195 mole) of 2-methyl-3(1-naphthylcarbonyl)nitrobenzene and 103 ml (0.784 mole) of DMF dimethyl acetal in 300 ml of DMF was heated under reflux for seventeen hours and then taken to dryness to give 2-(2-dimethylaminoethenyl)-3-(1-naphthylcarbonyl)nitrobenzene as an oil.