2-Amino-2',5-dichlorobenzophenone → 2-Amino-2',5-dichlorobenzophenone hydrazine
Reaction equation
[NH2:1][C:2]1[CH:16]=[CH:15][C:14]([Cl:17])=[CH:13][C:3]=1[C:4]([C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=1[Cl:12])=[O:5].O.[NH2:19][NH2:20]>C(O)COCCO>[NH2:19][NH2:20].[NH2:1][C:2]1[CH:16]=[CH:15][C:14]([Cl:17])=[CH:13][C:3]=1[C:4]([C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=1[Cl:12])=[O:5]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
In the manner given in Preparation 1, 2-amino-2',5-dichlorobenzophenone is refluxed with hydrazine hydrate in diethylene glycol to give 2-amino-2',5-dichlorobenzophenone hydrazine.
Sources & evidence
- ORD record
- ord-d54b9c03624b495ebbcbdc72bfaf9831
- Source dataset
- uspto-grants-1976_03
- Patent number
- US03941802
Reaction notes
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