Cyanuric chloride → 3-Chlorooctane

HRID 354263

Reaction equation

[CH3:1][CH2:2][CH:3](O)[CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].N1C(Cl)=NC(Cl)=NC=1[Cl:12]>>[Cl:12][CH:3]([CH2:4][CH2:5][CH2:6][CH2:7][CH3:8])[CH2:2][CH3:1]

Participants

Reactant 2

HCID 7954Cyanuric chloride

HCID 115273-Octanol

Product 1

HCID 335753-Chlorooctane

Procedure

Using a procedure analogous to that of Example 1, 81 g (0.522 mol) of 3-octanol is reacted with 62.1 g (0.337 mol) of cyanuric chloride over a period of 9 hours at a reaction temperature of 70° C. The liquid reaction phase after extraction with sodium hydroxide has the following composition:

Workup

customThe liquid reaction phase
extractionafter extraction with sodium hydroxide

Sources & evidence

ORD record: ord-a64555b8c0f043069480e86d2d585f4e
Source dataset: uspto-grants-2004_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06756513B2

Linked notes

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