Methyl Acrylate → HCID 15919806, compound

HRID 371894

Reaction equation

HRID 371894 reaction equation
[CH2:1]([NH2:17])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[C:18]([O:22][CH3:23])(=[O:21])[CH:19]=[CH2:20]>CO>[CH2:1]([NH:17][CH:19]([CH3:20])[C:18]([O:22][CH3:23])=[O:21])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

Participants

4

Reactant 2

HCID 7294Methyl AcrylateHCID 8926Hexadecylamine

Product 1

HCID 15919806HCID 15919806, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

66.4 g of hexadecylamine are dissolved in 250 ml of methanol. 27 ml of methyl acrylate are added and the mixture is left to stand overnight. After removal of the solvent by distillation the residue is recrystallised from ethyl acetate.

Workup

  1. waitthe mixture is left
  2. customAfter removal of the solvent
  3. distillationby distillation the residue
  4. customis recrystallised from ethyl acetate

Sources & evidence

ORD record
ord-7c99f89006944ecc9fb1dc936a498189
Source dataset
uspto-grants-1978_05
Patent number
US04088491

Linked notes

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