Hydroquinone → Dicumyl peroxide

HRID 380062Notes

Reaction equation

HRID 380062 reaction equation
C[O-].[Na+].[O-2].[Al+3].[O-2].[O-2].[Al+3].[C:9]1([CH:16]=[CH:15][C:13](O)=[CH:12][CH:11]=1)O.C[CH2:18][C:19]([O:23][O:24][C:25](OO)([CH2:27]C)[CH3:26])(OO)[CH3:20].CN(C)[C:33]1[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=1>ClCCl.C1(C)C=CC=CC=1>[C:19]([O:23][O:24][C:25]([C:33]1[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=1)([CH3:27])[CH3:26])([C:9]1[CH:16]=[CH:15][CH:13]=[CH:12][CH:11]=1)([CH3:20])[CH3:18]

Participants

8

Reactant 5

HCID 785HydroquinoneHCID 949N,N-DimethylanilineHCID 3672772Methyl ethyl ketone peroxideHCID 9989226AluminaHCID 10942334Sodium Methoxide

Product 1

HCID 6641Dicumyl peroxide

Reagents, catalysts & solvents 2

HCID 1140TolueneSolventHCID 6344DichloromethaneSolvent

Procedure

Sodium methoxide (NaOCH3), toluene (anhydrous), dichloromethane, hexanes, activated neutral aluminum oxide (60 to 50 mesh), hydroquinone, methyl ethyl ketone peroxide, dimethylaniline, dicumylperoxide were obtained from commercial sources and used as received.

Sources & evidence

ORD record
ord-d901dd241c564dd493adae2c78ed4c08
Source dataset
uspto-grants-2001_10
Patent number
US06300457B1

Reaction notes

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