Triethylamine → Triethylammonium trifluoromethanesulfonate

Reaction equation

[F:1][C:2]([F:8])([F:7])[S:3]([OH:6])(=[O:5])=[O:4].[CH2:9]([N:11]([CH2:14][CH3:15])[CH2:12][CH3:13])[CH3:10]>>[F:1][C:2]([F:8])([F:7])[S:3]([O-:6])(=[O:5])=[O:4].[CH2:9]([NH+:11]([CH2:14][CH3:15])[CH2:12][CH3:13])[CH3:10]

Participants

Reactant 2

HCID 8471Triethylamine2×

HCID 62406Trifluoromethanesulfonic acid2×

Product 1

HCID 14718426Triethylammonium trifluoromethanesulfonate

Procedure

Equimolar amounts of triethylamine and trifluoromethanesulfonic acid were weighed in a glove box under argon atmosphere. The weighed triethylamine and trifluoromethanesulfonic acid were mixed and stirred while being cooled by liquid nitrogen, thus obtaining a target ionic conductor.

Workup

temperaturewhile being cooled by liquid nitrogen
customthus obtaining a target ionic conductor

Sources & evidence

ORD record: ord-a75f31e657b84c399714d8636269916a
Source dataset: uspto-grants-2013_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08535849B2

Reaction notes

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