Santonox → HCID 13041335, compound

HRID 435491

Reaction equation

HRID 435491 reaction equation
[CH3:1][CH:2]([NH:4][C:5]([C:7](=O)C=CC1C=CC=C(Cl)C=1)=[O:6])[CH3:3].[Cl:18][C:19]1[CH:24]=[CH:23][CH:22]=[C:21]([C:25]([O:27]O)=O)[CH:20]=1.S(C1C(C)=CC(O)=C(C(C)(C)C)C=1)C1C(C)=CC(O)=C(C(C)(C)C)C=1>C(Cl)CCl>[CH3:1][CH:2]([NH:4][C:5]([CH:7]1[CH:25]([C:21]2[CH:22]=[CH:23][CH:24]=[C:19]([Cl:18])[CH:20]=2)[O:27]1)=[O:6])[CH3:3]

Participants

5

Reactant 3

HCID 7308SantonoxHCID 70297m-Chloroperbenzoic acidHCID 53986957N-(1-Methylethyl)-3-Chlorocinnamoylcarboxamide

Product 1

HCID 13041335HCID 13041335, compound

Reagents, catalysts & solvents 1

HCID 111,2-DichloroethaneSolvent

Procedure

This compound was prepared from N-(1-methylethyl)-3-chlorocinnamoylcarboxamide (22.4 g.), m-chloroperbenzoic acid (23.6 g.), 4,4'-thiobis(6-tert-butyl-m-cresol) (0.3 g.), and ethylene dichloride as described in Example 7, and purified by recrystallization from ether. The compound melted at 131°-133°, and weighed 14.5 g.

Workup

  1. custompurified by recrystallization from ether

Sources & evidence

ORD record
ord-d2d13e47b39349899f6b2d8a153831f9
Source dataset
uspto-grants-1983_08
Patent number
US04401832

Linked notes

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