2-Bromohexanoic acid → 6-Bromohexanoyl chloride

HRID 487038

Reaction equation

HRID 487038 reaction equation
[Br:1][CH:2]([CH2:6][CH2:7][CH2:8]C)C(O)=O.[C:10](Cl)(=O)[C:11]([Cl:13])=[O:12]>CN(C)C=O>[Br:1][CH2:2][CH2:6][CH2:7][CH2:8][CH2:10][C:11]([Cl:13])=[O:12]

Participants

4

Reactant 2

HCID 120132-Bromohexanoic acidHCID 65578Oxalyl chloride

Product 1

HCID 898486-Bromohexanoyl chloride

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

58.5 g of (0.3 moles) of 6 bromohexanoic acid and 85 ml of oxalyl chloride are placed in a 250-ml flask with a magnetic agitator. The mixture is agitated and 1 milliliter of dimethylformamide (DMF) is added.

Sources & evidence

ORD record
ord-b0c2c43ef3fd413fb7975f6bb0c6f238
Source dataset
uspto-grants-1994_03
Patent number
US05294463

Linked notes

Loading…