Phosphoric Acid → HCID 178527096, compound

A 5 L beaker was charged with 2 L of ion-exchanged water, and 252 g of lithium hydroxide was added to the beaker, and dissolved. After the addition of 364 g of vanadium pentoxide to the solution, the mixture was stirred for 1 hour. After the addition of 72 g of glucose and 692 g of 85% phosphoric acid to the mixture, the mixture was stirred for 1 hour to obtain a raw material mixture. The raw material mixture was supplied to a spray dryer (hot blast inlet temperature: 230° C., hot blast outlet temperature: 120° C.) to obtain a spray-dried product. The spray-dried product was placed in a saggar made of mullite, and calcined at 900° C. for 12 hours in a nitrogen atmosphere. The calcined product was disintegrated using a jet mill to obtain a lithium vanadium phosphate-carbon composite sample. FIG. 5 shows the particle size distribution measurement results for the lithium vanadium phosphate-carbon composite sample.

1. additionwas added to the beaker
2. dissolutiondissolved
3. stirringthe mixture was stirred for 1 hour
4. customto obtain a raw material mixture
5. customwas supplied to a spray dryer (hot blast inlet temperature: 230° C., hot blast outlet temperature: 120° C.)
6. customto obtain a spray-dried product
7. waitcalcined at 900° C. for 12 hours in a nitrogen atmosphere

ORD record

ord-7b8bf26b845c4118acfef9eb77432a86

Source dataset

uspto-grants-2016_09

DOI

10.6084/m9.figshare.5104873.v1

Patent number

US09437866B2