Hydrochloric Acid → HCID 19600186, compound
Reaction equation
[CH3:1][N:2]([CH2:4][C:5]1[O:13][C:12]2[CH2:11][CH2:10][N:9]([C:14](=[O:28])[C:15]3[CH:20]=[CH:19][C:18]([C:21]([C:23]4[O:24][CH:25]=[CH:26][CH:27]=4)=[O:22])=[CH:17][CH:16]=3)[CH2:8][C:7]=2[CH:6]=1)[CH3:3].[ClH:29]>CO.C(OCC)(=O)C>[ClH:29].[CH3:3][N:2]([CH2:4][C:5]1[O:13][C:12]2[CH2:11][CH2:10][N:9]([C:14](=[O:28])[C:15]3[CH:20]=[CH:19][C:18]([C:21]([C:23]4[O:24][CH:25]=[CH:26][CH:27]=4)=[O:22])=[CH:17][CH:16]=3)[CH2:8][C:7]=2[CH:6]=1)[CH3:1]Participants
5
Reactant 2
Product 1
Reagents, catalysts & solvents 2
Procedure
N,N-Dimethyl-[5-[4-(2-furoyl)benzoyl]-4,5,6,7-tetrahydrofuro[3,2-c]pyridin-2-ylmethyl]amine 0.148 g was dissolved in 2 ml of methanol; hydrogen chloride in ethyl acetate was added in excess, followed by stirring. This mixture was then concentrated and washed with diethyl ether to yield the desired product.